Recrystallization of 3-nitro-1,2,4-triazol-5-one from dimethylsu

Details Recrystallization of 3-nitro-1,2,4-triazol-5-one from dimethylsu Recrystallization of 3-nitro-1,2,4-triazol-5-one from dimethylsu

1989-07-26

1991-11-05

Stoll, Robert L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

C07D24912, C07D24914

Patent

active

H00009903

ABSTRACT:
The production of 3-nitro-1,2,4-triazol-5-one (NTO) having finely divided rticles of uniform size by dissolving conventionally produced large, jagged, rods of NTO in hot dimethylsulfoxide and then injecting the hot solution through a small orifice into methylene chloride at a temperature of from about -10.degree. C. to about 30.degree. C.

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