Recovery process for oxidation catalyst in the manufacture of ar

Catalyst – solid sorbent – or support therefor: product or process – Including ion exchanging – except zeolites or product thereof – For regenerating or rehabilitating catalyst or sorbent

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502 24, 502 27, 423 49, 423139, 562414, B01J 2034, B01J 3730, B01J 3868

Patent

active

059553944

ABSTRACT:
An improved separation process for the continuous catalytic oxidation of aromatic alkyls for the production of aromatic carboxylic acids in a liquid solvent medium, wherein the reactor product stream is withdrawn from the oxidation process, then separated to produce a product containing stream, mother liquor stream and a catalyst containing purge stream which is then passed through a filtration system and series of sorption vessels to remove the oxidation catalyst and separate the impurities from the catalyst. The solvent is then separated from the reaction by-products by conventional distillation methods. The solvent is recycled to the process while the reaction by-product residue is disposed of by incineration. The oxidation catalyst is eluted from the ion exchange columns and returned to the process.

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