Recovery of sodium and antimony values from spent ethylene glyco

Chemistry of inorganic compounds – Treating mixture to obtain metal containing compound – Group va metal or arsenic

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423208, C01B 2902

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active

041002539

ABSTRACT:
A process for recovering antimony and sodium compounds from antimony-containing spent ethylene glycol residues resulting from the manufacture of polyethylene-terephthalate polyester, which comprises combusting the spent glycol residues to produce an ash, and then contacting the ash with water to form an ash-water mixture having a liquid phase and a solid phase, the water-soluble sodium compounds being essentially contained in the liquid phase and the water-insoluble antimony compounds being essentially contained in the solid phase. The liquid phase and solid phase are then separated in order to recover therefrom sodium and antimony compounds, respectively.

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patent: 3554859 (1971-01-01), Murray
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patent: 3761568 (1973-09-01), Brink et al.
patent: 3840641 (1974-10-01), Wampfler et al.
Handbook of Chemistry and Physics, 43rd Edition (1961), pp. 536, 537, 650-653.

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