Recovery of products from toluenediisocyanate residues

Distillation: processes – separatory – With chemical reaction – Including step of adding catalyst or reacting material

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

203 98, 521160, 560358, 560360, B01D3/34

Patent

active

059024593

ABSTRACT:
There is now provided a method of recycling toluenediisocyanate residue resulting from the production of toluenediisocyanate by the reaction of toluenediamine by phosgenation in the presence of a solvent. In accordance with the teachings of the present invention, the toluenediisocyanate residue is treated at reflux with an alkanolamine to obtain an intermediary product which is distilled thereby giving rise to various products including but not limited to at least one component selected from toluenediamine, oxazolidone and hydroxyethylimidiazolidone. Preferably the alkanolamine employed is a monoethanolamine.

REFERENCES:
patent: 3404103 (1968-10-01), Matsudaira et al.
patent: 3658656 (1972-04-01), Adica et al.
patent: 3729386 (1973-04-01), Irwin et al.
patent: 4076577 (1978-02-01), Hetzel et al.
patent: 4480081 (1984-10-01), Rosin et al.
patent: 4654443 (1987-03-01), Marks et al.
patent: 4794194 (1988-12-01), Burgoyne et al.
patent: 5281629 (1994-01-01), Hoveaindt et al.
patent: 5298128 (1994-03-01), Hansdorf et al.
patent: 5314588 (1994-05-01), Zarnack et al.
patent: 5354369 (1994-10-01), Shimomura et al.
patent: 5498780 (1996-03-01), Kubota et al.
Perry et al "Distillation", 1965, p. 3.
"Decomposition of Polyurethane Foams by Alkanolamines," Kanaya and Takahashi, Journal of Applied Polymer Science, vol. 51, pp. 675-682 (1994).
"Preparation of Epoxy Hardeners from Waste Rigid Polyurethane Foam and Their Application," S. Xue et al., Journal of Applied Polymer Science, vol. 56, pp. 127-134 (1995).

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Recovery of products from toluenediisocyanate residues does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Recovery of products from toluenediisocyanate residues, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Recovery of products from toluenediisocyanate residues will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-243822

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.