Recovery of lignin and water soluble sugars from plant...

Chemistry: natural resins or derivatives; peptides or proteins; – Lignins or derivatives – Compound which includes phenolic hydroxy or oxygen...

Reexamination Certificate

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Reexamination Certificate

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07985847

ABSTRACT:
In one aspect, a process for treating woody plant material is provided, the process involving contacting the plant material with a continuous flow of an aqueous ethanol solution at elevated temperature and pressure under conditions that promote extraction of ethanol-soluble lignin from the plant material and retention of hemicellulose sugars, xylose and cellulose in the treated plant material solids. In another aspect, a process for extracting hemicellulose sugars from lignin-depleted plant material solids is provided, the process involving contacting lignin-depleted plant material with water at elevated temperature and pressure under conditions that promote extraction of hemicellulose sugars from the plant material; and recovering hemicellulose sugars from the liquid mixture.

REFERENCES:
patent: 3585104 (1971-06-01), Kleinert
patent: 4100016 (1978-07-01), Diebold et al.
patent: 4100106 (1978-07-01), Stefani et al.
patent: 4409032 (1983-10-01), Paszner et al.
patent: 4470851 (1984-09-01), Paszner et al.
patent: 4764596 (1988-08-01), Lora et al.
patent: 5196460 (1993-03-01), Lora et al.
patent: 5372939 (1994-12-01), Lastick et al.
patent: 5680995 (1997-10-01), Salminen
patent: 5681427 (1997-10-01), Lora et al.
patent: 5705216 (1998-01-01), Tyson
patent: 5788812 (1998-08-01), Agar et al.
patent: 5865948 (1999-02-01), Lora et al.
patent: 5879463 (1999-03-01), Proenca
patent: 6409841 (2002-06-01), Lombard
patent: 6660506 (2003-12-01), Nguyen et al.
patent: 6763947 (2004-07-01), Brooks
patent: 7109005 (2006-09-01), Eroma et al.
patent: 7189306 (2007-03-01), Gervais
patent: 7465791 (2008-12-01), Hallberg et al.
patent: 2002/0069987 (2002-06-01), Pye
patent: 2008/0029233 (2008-02-01), Wingerson et al.
patent: 2008/0032344 (2008-02-01), Fallavollita
patent: 2008/0295980 (2008-12-01), Hallberg et al.
patent: 2008/0299628 (2008-12-01), Hallberg et al.
patent: 200051888 (2001-02-01), None
patent: 84/03304 (1984-08-01), None
patent: 92/13849 (1992-08-01), None
patent: 96/41052 (1996-12-01), None
patent: 0210073 (2002-02-01), None
patent: 2007/051269 (2007-05-01), None
patent: 2007/129221 (2007-11-01), None
patent: 2008/144878 (2008-12-01), None
patent: 2008/144903 (2008-12-01), None
patent: 2009/003292 (2009-01-01), None
Blokhina, Olga et al., Antioxidants, Oxidative Damage and Oxygen Deprivation Stress: a Review; Annals of Botany, vol. 91, pp. 179-194 (2003), Helsinki University, Finland.
Aldrich Handbook of Fine Chemicals and Laboratory Equipment, (Sigma-Aldrich), pp. 1124-1125; (2003-2004) Australia-New Zealand.
PCT/NZ2007/000106 International Search Report; Australian Patent Office, 6 pages; (Sep. 9, 2007).
PCT/NZ2007/000106 Written Opinion; Australian Patent Office, 6 pages; (Sep. 9, 2007).
Balakshin, Mikhail Yu, et al., “Elucidation of the Structures of Residual and Dissolved Pine Kraft Lignins Using an HMQC NMR Technique,” J. Agric. Food Chem., vol. 51, pp. 6166-6127 (2003).
Berlin, Alex et al., “Inhibition of Cellulase, Xylanase and B-glucosidase Activities by Softwood Lignin Preparations,” Journal of Biotechnology, vol. 125, pp. 198-209 (2006).
Capanema, Ewellyn A. et al., “Quantitative Characterization of a Hardwood Milled Wood Lignin by Nuclear Magnetic Resonance Spectroscopy,” J. Agric. Food Chem., vol. 53, pp. 9639-9649 (2005).
Capanema, Ewellyn A. et al., “Structural Analysis of Residual and Technical Lignins by 1H-13C Correlation 2D NMR-Spectroscopy,” Holzforschung vol. 55, pp. 302-308 (2001).
Heindel, T.J. et al., “IPST Technical Paper Series No. 857,” Institute of Paper Science and Technology, Atlanta Georgia (May 2000).
Aristidou, Aritos, et al., “Metabolic engineering applications to renewable resource utilization,” Current Opinions Biotechnology, vol. 11, pp. 187-198 (2000).
Bakker, R.R., et al., “Biofuel production from acid-impregnated willow and switchgrass,” 2nd World Conference on Biomass for Energy Industry and Climate Protection, pp. 1467-1470, Rome Italy (May 10-14, 2004).
Boussaid, Abdel, et al., “Fermentability of the Hemicellulose-Derived Sugars from Steam-Exploded Softwood (Douglas Fir),” Biotechnology and Bioengineering, vol. 64, No. 3, pp. 284-289 (Aug. 5, 1998).
Brownell, Harold H. et al., “Steam pre-treatment of lignocellulosic material for enhanced enzymatic hydrolyssis” Biotechnology and Bioengineering, vol. 29, pp. 228-235 (Feb. 1987).
Chum, H.L. et al., “Organosolv Pretreatment for Enzymatic Hydrolysis of Poplars: I Enzyme Hydrolysis of Cellulosic Residues,” Biotechnology and Bioengineering, vol. 31, pp. 643-649 (May 1988).
Funaoka, M. et al., “Conversion of Native Lignin to a Highly Phenolic Functional Polymer and Its Separation From Lignocellulosics,” Biotechnology and Bioengineering, vol. 46, No. 6, pp. 545-552 (Jun. 20, 1995).
Garrote, G. et al., “Non-isothermal autohydrolysis of Eucalyptus wood,” Wood Scient and Technology, vol. 36, pp. 111-123 (2002).
Holtzapple, Mark T. et al., “The effect of ogranosolv pretreatment on the enzymatic hydrolysis of poplar,” Biotechnology and Bioengineering, vol. 26, pp. 670-676 (Jul. 1984).
Kim, S. et al., “Effect of structural features on enzyme digestibility of corn stover,” Bioresource Technololgy, vol. 97(4) pp. 583-591 (2006).
Kim, Tai Hyun et al., “Fractionation of corn stover by hot-water and aqueos ammonia treatment,” Bioresource Technology vol. 97, pp. 224-232 (2006).
Klinke, H.B. et al., “Inhibition of ethanol-producing yeast and bacteria by degradation products produced during pre-treatment of biomass.” Appl. Microbiol. Biotechnol. vol. 66, pp. 10-26 (2004).
Kubo, Satoshi et al., “Poly (Ethylene Oxide)/Organosolv Lignin Blends: Relationship between Thermal Properties, Chemical Structure, and Blend Behavior,” Macromolecules vol. 37, No. 18, pp. 6904-6911 (Jul. 31, 2004).
Lin, Yan et al., “Ethanol fermentation from biomass resources: current state and prospects,” Appl. Microbiol. Biotechnol. vol. 69, pp. 627-642 (2006).
Liu, Chaogang et al., “Partial flow of compressed-hot water through corn stover to enhance hemicellulose sugar recovery and enzymatic digestibility of cellulose,” Bioresource Technololgy, vol. 96, pp. 1978-1985 (Feb. 2006).
Lora, Jairo H. et al., “Recent Industrial Applications of Lignin: A Sustainable Alternative to Nonrenewable Materials.” Journal of Polymers and the Environment, vol. 10, Nos. 1-2, pp. 39-47 (Apr. 2002).
Mosier, Nathan et al., “Features of promising technologies for pretreatment of lignocellulosic biomass,” Bioresource Technology, vol. 96, pp. 673-686 (2005).
Nagle, Nicholas J. et al., “Efficacy of a hot washing process for pretreated yellow poplar to enhance bioethanol production,” Biotechnol. Prog., vol. 18, No. 4, pp. 734-738 (May 6, 2002).
Pan, Xuejun et al., “Biorefining of softwoods using ethanol organosolv pulping: preliminary evaluation of process streams for manufacture of fuel-grade ethanol andco-products,” Biotechnology and Bioengineering, vol. 90, No. 4, pp. 473-481 (May 20, 2005).
Rughani, Jagdish et al., “Combined Rapid-Steam Hydrolysis and Organosolv Pretreatment of Mixed Southern Hardwoods,” Biotechnolology and Bioengineering, vol. 33, pp. 681-686 (Feb. 1989).
Wyman, Charles E. et al., “Comparative sugar recovery data from laboratory scale application of leading pretreatment technologies to corn stover,” Bioresource and Technology, vol. 96, pp. 2026-2032 (Feb. 25, 2005).
Wyman Charles E. et al., “Coordinated development of leading biomass pretreatment technologies,” Bioresource and Technology, vol. 96, pp. 1959-1966 (Feb. 26, 2005).
Yang, Bin et al., “Effect of Xylan and Lignin Removal by Batch and Flowthrough Pretreatment on the Enzymatic Digestibility of Corn Stover Cellulos,.” Bioresource and Technology, vol. 86, No. 1, pp. 88-95 (Apr. 15, 2004).
Peng, Claudio A.,“Bioref

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