Recovery of caprolactam from process residues

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07D20112

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045826420

ABSTRACT:
This invention is a method to recover caprolactam from a combined stream of mother liquor from a caprolactam crystallizer and other lactam containing aqueous streams, the improvement comprising steam distilling the combined stream at a temperature of from between about 180.degree. C. to 235.degree. C. in the absence of any depolymerization agent such as phosphoric acid; so that the residue from the steam distilling remains fluid; relatively low levels of caprolactam remain in the residue; less residue is generated; the recovered caprolactam has improved high quality; and losses of caprolactam due to side reactions are reduced.

REFERENCES:
patent: 4107160 (1978-08-01), Dicoi
patent: 4148793 (1979-04-01), Danziger

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