Reagent and method for determining activity of retroviral protea

Chemistry: natural resins or derivatives; peptides or proteins; – Peptides of 3 to 100 amino acid residues – 6 to 7 amino acid residues in defined sequence

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530327, 530324, 435 23, A61K 3902

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active

050119109

ABSTRACT:
Novel fluorogenic substrates for retroviral protease, e.g. HIV protease, having the chemical structure X--Thr--Ile--Nle--Phe(Y)--Gln--Arg--NH.sub.2 wherein X is a fluorogenic group and Y is an acceptor for the fluorogenic group, and their use in a fluorometric method for the determination of retroviral protease is disclosed.

REFERENCES:
patent: 3384555 (1968-05-01), Guilbault et al.
Matayoshi et al., Novel Fluorogenic Substrates for Assaying Retroviral Proteases by Resonance Energy Transfer, Science, 1990, pp. 954-957.
Carmel and Yaron, Eur. J. Biochem. 87, 265-273 (1978).
Soler and Harris, Int. J. Peptide Protein Res. 32, 35-40 (1988).
Malfray and Brunier, Biochem. Biophys. Res. Commun. 143, 58-66 (1987).
Vencill et al., Biochemistry 24, 3149-3157 (1985).
Guilbault, Enzymatic Methods of Analysis, Pergamon Press, 1970, pp. 43-47.
Nashed et al., Biochem. Biophys. Res. Commun. 163, 1079-1085 (1989).
Hyland et al., Abstr. 2nd Int. Conf. Drugs Res. Immunologic and Infectious Disease, Aids New York Acad. Sci. I-20 (1989); Matayoshi, Ibid. I-26; Wang, Ibid. I-27.
Yaron et al., Anal. Biochem. 95, 228-235 (1979).

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