Reactor for producing a nitrile compound and method for...

Organic compounds -- part of the class 532-570 series – Organic compounds – Nitriles

Reexamination Certificate

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C558S327000

Reexamination Certificate

active

10940652

ABSTRACT:
A reactor for producing a nitrile compound from a carbon ring or heterocyclic compound having organic substituents by a gas phase reaction using a fluidized catalyst bed with ammonia and a gas containing oxygen. In a cylindrical fluidized catalyst bed having a diameter of 2.0 meters or greater, partial vaporization-type cooling tubes (the cooling medium is partially vaporized in the tubes) and complete vaporization-type cooling tubes (the cooling medium is completely vaporized in the cooling tubes) are disposed in a specific arrangement. Water containing ionic SiO2in 0.1 ppm or smaller and having an electric conductivity of 5 μS/cm or smaller is used as the cooling medium for the complete vaporization-type cooling tubes. The temperature of the reaction is easily stabilized and uniform distribution of temperature is obtained in the fluidized catalyst bed. Stable continuous operation is achieved for a long time in a commercial scale apparatus.

REFERENCES:
patent: 4544020 (1985-10-01), Chrysostome et al.
patent: 5700432 (1997-12-01), Tanaka et al.
patent: 6110440 (2000-08-01), Ohta et al.
patent: 6218484 (2001-04-01), Brown et al.
patent: 1113001 (2001-07-01), None
patent: 2 034 019 (1970-12-01), None
patent: WO 99/15484 (1999-04-01), None
Communication and European Search Report dated Aug. 11, 2004, for No. EP 02 02 8774.

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