Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing
Patent
1994-08-26
1995-07-25
Lone, Werren B.
Organic compounds -- part of the class 532-570 series
Organic compounds
Oxygen containing
568568, 568569, 568910, C07C40904, C07C 2710
Patent
active
054363756
ABSTRACT:
Tertiary butyl hydroperoxide and tertiary butyl alcohol are prepared from isobutane and oxygen in a vertical reactor by sparging a mixture of isobutane with oxygen to the bottom of the reactor, by charging a reaction mixture recycle stream to the reactor above the sparge point, by centrally charging a downwardly flowing stream of cooled fresh isobutane to the top of the reactor to induce central downflow of the fresh isobutane annular and upflow of the sparged mixture and the recycle stream, by withdrawing a liquid product stream adjacent the top of the reactor, by withdrawing a vapor product stream from the top of the reactor, by condensing entrained liquids in the vapor product, by recycling the condensed liquids and by recovering the liquid product stream.
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Preston Kyle L.
Thomas Karen A.
Bailey James L.
Lone Werren B.
Priem Kenneth R.
Ries Carl G.
Texaco Chemical Inc.
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