Quantitative evaluation of emulsion stability based on...

Data processing: measuring – calibrating – or testing – Measurement system – Performance or efficiency evaluation

Reexamination Certificate

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C204S556000

Reexamination Certificate

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11302800

ABSTRACT:
A method for quantitative evaluation of emulsion stability using Critical Electric Field (CEF) determinations over a range of conditions, such as a range of temperatures, demulsifier compositions, or demulsifier concentrations. The method includes determining the CEF for a series of emulsions that differ substantially only in their internal phase volume ratio. A plot of CEF values as a function of the inverse of the internal phase volume ratio is characterized by a linear slope. Using the slope, a theoretical CEF value can be determined by extrapolating to where the inverse of the internal phase volume ratio is about one. The slope for a given emulsion series is associated with the relative energy barrier to flocculation and the theoretical critical electric field for a given emulsion series is associated with the relative energy barrier to coalescence. Comparative studies are performed using this method.

REFERENCES:
patent: 4624763 (1986-11-01), Chimenti
patent: 4981569 (1991-01-01), Schugerl et al.
patent: 5283001 (1994-02-01), Gregoli et al.
patent: 5435920 (1995-07-01), Penth
patent: 5580464 (1996-12-01), Bailes
patent: 5582700 (1996-12-01), Bryning et al.
patent: 5607574 (1997-03-01), Hart
patent: 5868939 (1999-02-01), Oder et al.
patent: 6068054 (2000-05-01), Bragg
patent: 6860979 (2005-03-01), Sams
patent: 2002/0101244 (2002-08-01), Dahms
patent: 2003/0206024 (2003-11-01), Murphy, Jr. et al.
Journal of Membrane Science vol. 128, May 1997; pp. 1-6; XP004068489; “Break-down of liquid membrane emulsion under high electric field”; Lu Gang, Lu QiongHua, Li PanSheng.
Proceedings of 2002 IEEE 14thInternational Conference on Dielectric Liquids (ICDL 2002), Graz (Austria), Jul. 7-12, 2002; “Instability of electrically stressed water droplets in oil”; Gunnar Berg, Lars E. Lundgaard, et al.
Colloid and Surfaces A; pp. 33-47; “Crude oil emulsions in high electric fields as studied by dielectric spectroscopy. Influence of interaction between commercial and indigenous surfactants”; Harald Fordedal, et al.
Journal of Colloid and Interface Science vol. 225, pp. 494-504; May 2000; “Quantitative Determination of Asphaltenes and Resins in Solution by Means of Near-Infrared Spectroscopy. Correlations to Emulsion Stability”; Harald Kallevik, et al.
The PCT International Search Report; Apr. 2005.
PCT/US2005/045261, International Preliminary Report on Patentability Jun. 21, 2007.
Kallevik H, Olav M Kvalheim and Johan Sjöblom, Quantitative determination of asphaltenes and resins in solution by means of near-infrared spectroscopy. Correlations to emulsion stability; Journal of Colloid and Interface Science 494-504 (2000), May 25, 1999, Staoil R&D Centre, Rotvoll, N-7005 Trondheim, Norway and Department of Chemistry, University of Bergen Allegaten 41 41, N-5007 Bergen, Norway.
Fordedal Harald, Yannick Schildberg, Johan Sjöblom and Jean-Luc Volle: Crude oil emulsions in high electric fields as studied by dielectric spectroscopy. Influence of interaction between commercial and indigenous surfactants, Colloids and Surfaces A: Physicochemical and Engineering Aspects 106 (1196 33-47Mar. 10, 1995.
PCT International Preliminary Report on Patentability Jun. 21, 2007.

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