Quantification of the munitions, HMX, RDX, and TNT in waste wate

Details Quantification of the munitions, HMX, RDX, and TNT in waste wate Quantification of the munitions, HMX, RDX, and TNT in waste wate

1979-02-02

1981-02-24

Adee, John

Chemistry: physical processes

Physical processes

Crystallization

210656, B01D 1508

Patent

active

042525373

ABSTRACT:
Disclosed is a liquid chromatography process for the quantitative determination of nitro-amines and nitro-aromatics in liquid samples, which comprises directly injecting a liquid sample containing these compounds onto a liquid chromatography column, separating the compounds on the column by elution, and then monitoring the ultra-violet absorbance of the resulting eluant. The instant process finds particular application in the quantitative detection of munitions, such as HMX, RDX, TNT, and their degradation products, in aqueous effluent streams.

REFERENCES:
patent: 3884802 (1975-05-01), Spaans
patent: 4108604 (1978-08-01), Heller
patent: 4157299 (1979-06-01), Landownr
The Determination of Selected Munitions and Their Degradation Products Us High Performance Liquid Chromatography by Meier et al., Published by the American Chemical Society from 4th Joint Conference of Sensing of Envioronmental Pollutants, Published Mar. 1, 1978, Conference Nov. 6-11, 1977.
Introduction to Modern Liquid Chromatography by Snyder and Kirkland, John Wiley and sons, N.Y., N.Y., pp. 142-144, 200-203, 227-229, 469 and 198.
Thin Layer Chromatography an Annolated Bibliography, 1964-1968, pp. 142-145, by Haywood, Ann Arbor Science Publishers, Ann Arbor, Mich., 1968.

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