Purification of trehalose dimycolates

Inductor devices – Relatively movable coils – Angularly movable

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536119, C07H 106

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active

045799458

ABSTRACT:
A method of purifying crude trehalose dimycolates (TDM) is disclosed which comprises dissolving crude TDM in a solvent and then subjecting said solution to a low pressure silica gel column operating at a pressure between about 10 and 300 psi wherein the silica gel comprises particles in the range of between about 15 and 63 microns. The product of this process is also disclosed.

REFERENCES:
patent: 4307229 (1981-12-01), Liav et al.
patent: 4340588 (1982-07-01), Woodard

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