Purification of N-acetyl aminophenols

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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252402, 564 4, C07C10338

Patent

active

044749856

ABSTRACT:
A process for increasing the color-free shelf life of a crude N-acetyl aminophenol prepared by the acetylation of an aminophenol wherein the N-acetyl aminophenol contains color-forming impurities which are the products of oxidation of the aminophenol and other side reactions. The process comprises dissolving the crude N-acetyl aminophenol in a solvent containing a reducing agent, heating the solution at about the boiling point, crystallizing the N-acetyl aminophenol from the solution, washing the crystalline N-acetyl aminophenol with solvent containing reducing agent and thereafter separating and drying the crystalline N-acetyl aminophenol.

REFERENCES:
patent: 2625557 (1953-01-01), Cottle et al.
patent: 2654722 (1953-10-01), Young et al.
patent: 2799692 (1957-07-01), Croxall et al.
patent: 2822370 (1958-02-01), Cottle et al.
patent: 2945870 (1960-07-01), Young
patent: 2998450 (1961-08-01), Wilbert et al.
patent: 3042719 (1962-07-01), Hahn et al.
patent: 3081321 (1963-03-01), Young
patent: 3081322 (1963-03-01), Young
patent: 3113150 (1963-12-01), Young
patent: 3458574 (1969-07-01), Anselm et al.
patent: 3748358 (1973-07-01), Baron
patent: 3781354 (1973-12-01), Kosak
patent: 3917695 (1975-11-01), Schulman et al.

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