Purification of factor VIII with insoluble matrix having free su

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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424101, C07G 700, A61K 3516, A61K 3514

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045782180

ABSTRACT:
Factor VIII is purified by adsorption onto a insoluble matrix having free sulphate groups, such as dextran sulphate, and selective elution therefrom.
A suitable eluant for the purification of the von Willebrand protein (Factor VIIIR:vWp) is citrate buffer, pH 6.85, containing 0.47 M sodium chloride and 2.14 mM calcium chloride.
A suitable eluant for the purification of the Factor VIII complex (Factor VIIIR:Ag, Factor VIIIR:vWp and Factor VIII:C) is citrate buffer at pH value between 6.2 and 7.3 containing 1.0 M glycine, 2.14 mM calcium chloride and 0.5 M sodium chloride at +4.degree. C.

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Introduction to Modern Biochemistry, 3rd Ed. Karlson (1970), pp. 326-327.

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