Purification of dialkylbenzene dihydroperoxide

Details Purification of dialkylbenzene dihydroperoxide Purification of dialkylbenzene dihydroperoxide

1969-07-25

1977-01-04

Helfin, Bernard

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260610B, 203 14, C07C17902

Patent

active

040013383

ABSTRACT:
An improved method for separating para-dialkylbenzene monohydroperoxide from crude solid para-dialkylbenzene dihydroperoxide which comprises treating the solid dihydroperoxide with a liquid hydrocarbon to form a mixture, heating the mixture to a temperature of at least about 60.degree. C., cooling the mixture to below about 30.degree. C. and filtering or otherwise physically separating the solid dihydroperoxide.

REFERENCES:
patent: 2715646 (1959-12-01), Hawkins et al.
patent: 2915557 (1955-08-01), Kreps et al.
patent: 3190923 (1965-06-01), Sodomann et al.

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