Purification of acetic acid from wood acetylation process

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof

Reexamination Certificate

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Reexamination Certificate

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07612232

ABSTRACT:
A method of purifying acetic acid containing terpene and terpenoid impurities, includes: (a) supplying acetic acid containing terpene or terpenoid impurities and water to a distillation column; (b) azeotropically removing terpene or terpenoid impurities from the mixture of acetic acid and water supplied to the column as distillate; and (c) withdrawing a product stream from the column comprising acetic acid purified of terpene or terpenoid impurities. The method is particularly effective for purifying acetic acid recovered from a wood purification process.

REFERENCES:
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patent: 4804384 (1989-02-01), Rowell et al.
patent: 5160412 (1992-11-01), Berg
patent: 7355066 (2008-04-01), Johnson et al.
patent: 0 213 252 (1987-03-01), None
patent: 0680810 (1995-11-01), None
International Search Report and Written Opinion.

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