Purification and activity assurance of precipitated heterologous

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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424 85, 435 68, 435 70, 4351723, 435240, 435241, 435948, 436548, C07G 700

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045185263

ABSTRACT:
A process for isolating and purifying a precipitated heterologous protein from a host cell culture, including treating the host cell culture with a buffered solution of ionic strength suitable to solubilize most of the host protein but in which refractile heterologous protein is substantially insoluble, and disrupting the cells to form a supernatant and an insoluble fraction; treating the insoluble fraction with a strongly denaturing solution to solubilize the refractile heterologous protein; and recovering renatured heterologous protein.

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patent: 4462940 (1984-07-01), Hanisch et al.
Goeddel et al., Nature, vol. 281, pp. 544 to 548 (Oct. 18, 1979).
Kleid et al., Science, vol. 214, pp. 1125 to 1129 (Dec. 4, 1981).
Williams et al., Science 215, 687-688 (1982).
Goeddel et al., Proc. Natl. Acad. Sci. USA 76, 106-110 (1979).
Wetzel et al., Biochemistry 19, 6096-6104 (1980).
Wetzel et al., Gene 16, 63-71 (1981).
Ullmann et al., Biochem. Biophys. Res. Commun. 35, 35-42 (1969).

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