Pulsed and gated multi-mode microspectrophotometry device and me

Radiant energy – Luminophor irradiation

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2504591, 356318, G01N 2164

Patent

active

052528340

ABSTRACT:
A short pulse of laser excitation and a synchronized gating time control of a fluorescence spectrograph detector are combined with a microscope, precise focusing and delivery optics, multi-mode illumination means, cooling, and temperature controls to form a new microspectrophotometry system. The gating control can block detection of any unwanted excitation radiation, such as nearly instantaneous (within 10.sup.-12 seconds) emissions after the sample is pulse excited and delayed emissions (after 10.sup.-7 seconds) after the sample is pulse excited. The gating also allows delayed emissions to be separately isolated. The microscopic focusing, pulse excitation and time segregation of detected emissions achieves a new level of precision in the detected structural spectra and property measurements not generally achievable for composite samples by prior art methods and devices.

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Watson et al., "Simplification of Spectra by Electro-Optic Gating of the Radiant Emission from Laser-Produced Plasmas", J. Phys. E, 10 (12), 1977, pp. 1227-1228.
Moenke, "Uber den Stand der Mikro-Emissions-Spektralanalyse mit Feskorperlasern", Messtechnik, Jan. 1968, pp. 13-18.
Rasberry, "Laser Probe Excitation in Spectrochemical Analysis. I: Characteristics of the Source", Appl. Opt. 6(1), Jan. 1967, pp. 81-86.

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