Propylene oxide purification by extractive distillation

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

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203 14, 203 78, 203 84, 549541, B01D 340, C07D30132

Patent

active

051164663

ABSTRACT:
An extractive distillation agent consisting essentially of 1-methyl-2-pyrrolidone is fed to an extractive distillation column used for the distillation of propylene oxide contaminated with water, acetone and methanol to obtain an overhead distillate fraction consisting of essentially anhydrous propylene oxide contaminated with reduced quantities of acetone and methanol, and a heavier bottoms distillation fraction containing substantially all of the 1-methyl-2-pyrrolidone, water and acetone and some of the methanol introduced into the distillation column.

REFERENCES:
patent: 3838020 (1974-09-01), Kageyama et al.
patent: 4369096 (1983-01-01), Seifert et al.
patent: 4971661 (1990-12-01), Meyer et al.

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