Production of tetrafluorammonium bifluoride and tetrafluorammoni

Details Production of tetrafluorammonium bifluoride and tetrafluorammoni Production of tetrafluorammonium bifluoride and tetrafluorammoni

1978-02-21

1979-07-10

Peters, G. O.

Chemistry of inorganic compounds

Boron or compound thereof

423468, 423470, C01B 3506, C01C 116

Patent

active

041608119

ABSTRACT:
The compound NF.sub.4 MF.sub.6 where M is a Group V metalloid is reacted with a fluoride of sodium to yield tetrafluorammonium bifluoride in solution with hydrogen fluoride and a precipitate of the formula NaMF.sub.6. The preferred metaloid is antimony. The formed tetrafluorammonium bifluoride may be converted to NF.sub.4 BF.sub.4 by reaction with BF.sub.3.

REFERENCES:
christe et al., "Annual Report Inorg. Halogen Oxidizer Research", R 9881, Off. Nav. Research, 4-1976, pp. 1-19 & A6-A-35.
Christe et al., "Annual Report Inorg. Halogen Oxidizer Res.", R 9662, Off. Nav. Res. 5.1975, Appendix B.

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