Production of tetrabasic lead sulfate from solid state...

Chemistry of inorganic compounds – Sulfur or compound thereof – Oxygen containing

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C429S227000, C429S228000, C029S623100, C029S623500

Reexamination Certificate

active

07459140

ABSTRACT:
A solid state reaction method for the production of tetrabasic lead sulfate includes the steps of mixing a stoichiometric mixture of 4PbO and PbCO3and H2SO4and heating the stoichiometric mixture of 4PbO and PbCO3and H2SO4at a temperature between 500 and 700° C. for 3 to 8 hours. The method also includes the steps of deagglomerating and sieving resulting tetrabasic lead sulfate.

REFERENCES:
patent: 1572586 (1926-02-01), Weir
patent: 2159226 (1939-05-01), Reid
patent: 2165944 (1939-07-01), Scott
patent: 2182479 (1939-12-01), Johnstone
patent: 2717903 (1955-09-01), Ruth
patent: 3001013 (1961-09-01), Stanton
patent: 3104946 (1963-09-01), Veal
patent: 3169890 (1965-02-01), Voss et al.
patent: 3173810 (1965-03-01), Voss et al.
patent: 3186871 (1965-06-01), Donohue
patent: 3194685 (1965-07-01), Malloy
patent: 3252764 (1966-05-01), Bruno, Jr.
patent: 3384458 (1968-05-01), McCarthy et al.
patent: 3398024 (1968-08-01), Barnes et al.
patent: 3419431 (1968-12-01), Michaels
patent: 3449166 (1969-06-01), Jache
patent: 3480478 (1969-11-01), Sohn et al.
patent: 3702265 (1972-11-01), Snyder et al.
patent: 3734694 (1973-05-01), McCoy
patent: 3747560 (1973-07-01), Roberts et al.
patent: 3765943 (1973-10-01), Biagetti
patent: 3770507 (1973-11-01), Weissman et al.
patent: 3887693 (1975-06-01), Escribano Nevado et al.
patent: 3894886 (1975-07-01), Pankow et al.
patent: 3899349 (1975-08-01), Yarnell
patent: 3942433 (1976-03-01), Wohlfarter
patent: 3951688 (1976-04-01), Pankow et al.
patent: 3974026 (1976-08-01), Emson et al.
patent: 4019431 (1977-04-01), Bastgen
patent: 4020882 (1977-05-01), Foulkes
patent: 4024055 (1977-05-01), Blann
patent: 4050482 (1977-09-01), Ching et al.
patent: 4064725 (1977-12-01), Hug et al.
patent: 4110519 (1978-08-01), Nilsson
patent: 4140589 (1979-02-01), Hradcovsky et al.
patent: 4143218 (1979-03-01), Adams et al.
patent: 4212179 (1980-07-01), Juergens
patent: 4232100 (1980-11-01), Magnusson et al.
patent: 4315829 (1982-02-01), Duddy et al.
patent: 4323470 (1982-04-01), Mahato et al.
patent: 4324768 (1982-04-01), Sugahara et al.
patent: 4326017 (1982-04-01), Will
patent: 4336236 (1982-06-01), Kolakowski et al.
patent: 4346022 (1982-08-01), Wolcott et al.
patent: 4346151 (1982-08-01), Uba et al.
patent: 4383011 (1983-05-01), McClelland et al.
patent: 4387142 (1983-06-01), Lindholm et al.
patent: 4388210 (1983-06-01), Parker
patent: 4407911 (1983-10-01), Hooke
patent: 4414295 (1983-11-01), Uba
patent: 4415410 (1983-11-01), Reich
patent: 4421832 (1983-12-01), Uba
patent: 4422917 (1983-12-01), Hayfield
patent: 4475453 (1984-10-01), Davis
patent: 4501669 (1985-02-01), Hakansson et al.
patent: 4547443 (1985-10-01), Rowlette et al.
patent: 4551401 (1985-11-01), Wilson
patent: 4606982 (1986-08-01), Nelson et al.
patent: 4618478 (1986-10-01), McKinney
patent: 4637966 (1987-01-01), Uba et al.
patent: 4648177 (1987-03-01), Uba et al.
patent: 4656706 (1987-04-01), Mahato et al.
patent: 4697511 (1987-10-01), Davis et al.
patent: 4705602 (1987-11-01), Dahl
patent: 4707272 (1987-11-01), Kistler
patent: 4758372 (1988-07-01), Eirich et al.
patent: 4780379 (1988-10-01), Puester
patent: 4867886 (1989-09-01), Botkins, Jr.
patent: 4900643 (1990-02-01), Eskra et al.
patent: 4902532 (1990-02-01), Seo
patent: 5002700 (1991-03-01), Otagawa et al.
patent: 5021166 (1991-06-01), Torpey
patent: 5045086 (1991-09-01), Juergens
patent: 5047300 (1991-09-01), Juergens
patent: 5091273 (1992-02-01), Hug et al.
patent: 5092404 (1992-03-01), Falsk et al.
patent: 5096611 (1992-03-01), Matthew et al.
patent: 5120620 (1992-06-01), Nelson et al.
patent: 5198313 (1993-03-01), Juergens
patent: 5252105 (1993-10-01), Witherspoon et al.
patent: 5273554 (1993-12-01), Vyas
patent: 5290359 (1994-03-01), Coonen et al.
patent: 5302476 (1994-04-01), Kao et al.
patent: 5368961 (1994-11-01), Juergens
patent: 5382482 (1995-01-01), Suga et al.
patent: 5443601 (1995-08-01), Doeff et al.
patent: 5447809 (1995-09-01), Hafner et al.
patent: 5660600 (1997-08-01), Vyas
patent: 5871862 (1999-02-01), Olson
patent: 5958621 (1999-09-01), Kao
patent: 5998062 (1999-12-01), Olson
patent: 6014798 (2000-01-01), Nitsche et al.
patent: 6168661 (2001-01-01), Dinkelman
patent: 6274274 (2001-08-01), Schaeffer et al.
patent: 6442811 (2002-09-01), Dawood et al.
patent: 6454977 (2002-09-01), Kwok et al.
patent: 6755874 (2004-06-01), Chen et al.
patent: 7338647 (2008-03-01), Huang et al.
patent: 2002/0124388 (2002-09-01), Chen et al.
patent: 2004/0121233 (2004-06-01), Klein et al.
patent: 2004/0234852 (2004-11-01), Klein et al.
patent: 2005/0207969 (2005-09-01), Flores-Lira et al.
patent: 196507 (1986-10-01), None
patent: 0 540 229 (1993-05-01), None
patent: 0707718 (1996-04-01), None
patent: 8801559 (1988-04-01), None
patent: 723018 (1932-04-01), None
patent: 1014694 (1965-12-01), None
patent: 58-147961 (1983-09-01), None
patent: 59-101773 (1984-06-01), None
patent: 63-269456 (1988-11-01), None
patent: WO 8200258 (1982-02-01), None
patent: WO 02/069418 (2002-09-01), None
Grugeon-Dewaele, S., Laruelle, S., Joliveau-Vallat, F., Torcheux, Delahaye-Vidal, A., “Synthesis and Electrochemical Performances of Tribasic and Tetrabasic Lead Sulfates Prepared by Reactive Grinding”, Journal of Power Sources 72, 1998, pp. 126-131.
Vilhunen, J.K., Hornytzkyj, S. and Tummavuori, J. “The Influence of the Raw Material and Production Method on the Morphology, Microstructure, Chemical and Phase Composition of Tetrabasic Lead Sulfate Pastes”, Journal of Power Sources, vol. 39, 1992, pp. 59-65.
Pavlov, D. and Kapkov, N., “Lead-Acid Battery Pastes Containing 4Pb0—PbS04Pb3O4”, J. Electrochemical Society, vol. 137, No. 1, Jan. 1990, pp. 16-28.
Yarnell, C.F. and Weeks, M.C., “The Oxidation of Tetrabasic Lead Sulfate to Lead Dioxide in the Positive Plate of the Lead-Acid Battery”, Journal of the Electrochemical Society, Jan. 1979, vol. 126, No. 1, pp. 7-11.
McCabe, W.L. and Smith, J.C., “Unit Operations of Chemical Engineering” third edition, McGraw-Hill Book Company, 1976, 5 pages.
Pavlov, D. and Papazov, G., “Dependence of the Properties of the Lead-Acid Battery Positive Plate Paste on the Processes Occurring During Its Production” Journal of Applied Electrochemistry, vol. 6, No. 4, Jul. 1976, pp. 339-345.
Biagetti, R.V. and Weeks, M.C., “Tetrabasic Lead Sulfate as a Paste Material for Positive Plates”, Bell System Technical Journal, Sep. 1970, vol. 49, No. 7, pp. 1305-1319.
Burbank, J., “Anodic Oxidation of the Basic Sulfates of Lead” Journal of the Electrochemical Society, vol. 113, No. 1, Jan. 1966, pp. 10-14.
Grugeon-Dewaele, S.; Laruelle, S.; Joliveau-Vallat, F.; Torcheux, L.; Delahaye-Vidal, A.; “Synthesis and electrochemical performances of tribasic and tetrabasic lead sulfates prepared by reactive grinding”; Journal of Power Sources; vol. 72 (1998); pp. 126-131.
V. Lliev et al., “The Influence of PbO Modification on the Kinetics of the 4Pb).PbS04 Lead-acid Battery Paste Formation”, Journal of Applied Electrochemistry, vol. 9 (1979), pp. 555-562.
Search Report by European Patent Office for International Application No. PCT/IB2005/002373; date of mailing Oct. 24, 2005.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Production of tetrabasic lead sulfate from solid state... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Production of tetrabasic lead sulfate from solid state..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Production of tetrabasic lead sulfate from solid state... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-4044287

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.