Production of spheroidal alumina shaped articles

Plastic and nonmetallic article shaping or treating: processes – Formation of solid particulate material directly from molten...

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252448, 252463, 252464, 252465, 264 56, B01J 3702

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042737354

ABSTRACT:
Spheroidal alumina shaped articles are prepared by dispersing an ungelled admixture of an alumina sol and hexamethylenetetramine, in the form of droplets, into a liquid forming medium which is but very slightly miscible with water, said medium being at a temperature of between about 50.degree. and 105.degree. C., next aging the alumina spheres thus shaped at a temperature greater than about 105.degree. C. at superatmospheric pressure, then secondarily aging said alumina spheres in a basic medium, and thence washing, drying and calcining said aged alumina spheres.
The resultant shaped articles are useful, e.g., catalysts or catalyst carriers/supports.

REFERENCES:
patent: 2620314 (1969-05-01), Hoekstra
patent: 3442821 (1969-05-01), Hilfman
patent: 3600129 (1971-08-01), Vesely et al.

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