Production of sodium aluminum hydride

Details Production of sodium aluminum hydride Production of sodium aluminum hydride

1971-03-18

1976-05-25

Carter, Herbert T.

Chemistry of inorganic compounds

Hydrogen or compound thereof

C01B 100

Patent

active

039594548

ABSTRACT:
In the production of sodium aluminum hydride by reaction of an aluminum chloride etherate with sodium hydride in an inert liquid dispersing agent, the improvement which comprises using as said sodium hydride reagent coarse-grained sodium hydride which is first ground in said dispersing agent to a particle size less than about 12 microns; preferably the inert dispersible agent is tetrahydrofurane or a lower alkyl ether of a lower alkylene glycol, whereupon the resulting sodium aluminum hydride dissolves in the reaction medium.

REFERENCES:
patent: 2550985 (1951-05-01), Finholt
patent: 2900224 (1959-08-01), Hinckley et al.
patent: 3222288 (1965-12-01), Hansley et al.

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