Production of reactive sintered nickel aluminide material

Specialized metallurgical processes – compositions for use therei – Compositions – Consolidated metal powder compositions

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75249, 419 23, 419 34, 419 45, 419 46, 419 57, 419 58, 419 68, 420460, B22F 300

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active

047625589

ABSTRACT:
Reactive sintering process for producing a shaped body containing the nickel aluminide compound Ni.sub.3 Al, which comprises sintering a compacted shaped mass containing an intimate mixture of substances, e.g. including elemental nickel powder and elemental aluminum powder in a stoichiometric atomic ratio generally corresponding to the compound Ni.sub.3 Al, by heating the mass, e.g. in a vacuum, to an elevated sintering temperature, e.g. 500-750.degree. C., sufficiently to initiate an exothermic reaction, and at a heating rate sufficiently for consequent progressive generation of a transient liquid below the melting point of the aluminum powder and at the corresponding eutectic temperature, and upon initiation of the exothermic reaction continuing the sintering sufficiently to form a densified shaped body containing the nickel aluminide compound Ni.sub.3 Al, and having a porosity of at most about 8%, or alternatively having an essentially fully densified structure where the heating is carried out under simultaneously applied mechanical pressure for hot isostatic compaction of the compacted shaped mass.

REFERENCES:
patent: 2755184 (1956-07-01), Turner et al.
patent: 4609528 (1986-09-01), Chang et al.
patent: 4613368 (1986-09-01), Chang et al.
patent: 4676829 (1987-06-01), Chang et al.

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