Production of rare earth compounds

Chemistry of inorganic compounds – Rare earth compound

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423419R, C01F 1700

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044977859

ABSTRACT:
A method for preparing high-density particles of rare earth carbonate comprises precipitating rare earth ions with aqueous carbonate or bicarbonate ions, in the presence of rare earth carbonate crystals, and separating the resulting precipitate. The method can be conducted to prepare individual batches or, alternatively, a continuous precipitation method can be used, wherein rare earth and carbonate or bicarbonate ions are mixed at a controlled rate to maintain an optimum pH condition. High-density rare earth oxide is obtained by calcining the precipitate.

REFERENCES:
patent: 3401008 (1968-09-01), Head
patent: 3446574 (1969-05-01), Head
patent: 3573886 (1971-04-01), Geotzinger et al.
patent: 3692671 (1972-09-01), Recht et al.
M. W. Woyski and R. E. Harris, "The Rare Earths and Rare-Earth Compounds," in I. M. Kolthoff and P. J. Elving (Eds.), Treatise on Analytical Chemistry, Part II, vol. 8, John Wiley & Sons, Inc., New York, 1963, p. 16.

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