Plastic and nonmetallic article shaping or treating: processes – Formation of solid particulate material directly from molten... – By vibration or agitation
Patent
1991-08-05
1993-12-14
Theisen, Mary Lynn
Plastic and nonmetallic article shaping or treating: processes
Formation of solid particulate material directly from molten...
By vibration or agitation
264 5, 264 13, B29B 910
Patent
active
052699803
ABSTRACT:
A process for producing spherical polymer particles which may be either monodisperse of a predetermined and controlled size, or polydisperse, using a liquid atomization technique. The process includes an aerosol generator to create a stream or multiple streams of liquid droplets sprayed into a thermal reactor. The aerosol generator sprays the feed solution which comprises liquid organic monomers or semi-polymerized monomers, a polymerization catalyst and optionally, a solvent, into the thermal reactor environment. The solvent evaporates allowing polymerization reactions to commence. Polymerization may proceed by a variety of methods. Polymerization is completed during the flight-time of the droplets and the solid polymer particles are collected at the bottom of the reactor. The size of the particles in every batch may be predetermined and controlled by fine tuning the aerosol generator's configuration or operational parameters to adjust the size of the droplets of the feed solution being sprayed into the reactor. In one variation, the feed solution to the aerosol generator may be a polymer dissolved in an appropriate solvent. The aerosol generator then sprays the polymer solution in the thermal reactor to generate particles by evaporating the solvent.
REFERENCES:
patent: 2379237 (1945-06-01), Jenkins
patent: 2595852 (1952-05-01), Hopper
patent: 2790201 (1957-04-01), Eilbracht et al.
patent: 2968833 (1961-01-01), DeHaven et al.
patent: 3060510 (1962-10-01), Fischer et al.
patent: 3194781 (1965-07-01), Hodberg et al.
patent: 3203916 (1965-08-01), Veet
patent: 3215663 (1965-11-01), Weisberg
patent: 3372153 (1968-03-01), Turner et al.
patent: 3373232 (1968-03-01), Wise et al.
patent: 3397258 (1968-08-01), Williams
patent: 3422049 (1969-01-01), McClain
patent: 3431249 (1969-03-01), Bohrer et al.
patent: 3561003 (1971-02-01), Lanham et al.
patent: 3579721 (1971-05-01), Kaltenbach
patent: 3719733 (1973-03-01), Rakestraw et al.
patent: 3895035 (1975-07-01), Berg et al.
patent: 3896196 (1975-07-01), Dickey et al.
patent: 3923707 (1975-12-01), Berg et al.
patent: 3929934 (1975-12-01), Moore et al.
patent: 3968319 (1976-07-01), Mani et al.
patent: 3970633 (1976-07-01), Miller et al.
patent: 3993857 (1976-11-01), Smolinski et al.
patent: 3998778 (1976-12-01), Berg et al.
patent: 4052544 (1977-10-01), Kehl et al.
patent: 4076883 (1978-02-01), Dittrich
patent: 4158092 (1979-06-01), Botsch et al.
patent: 4185001 (1980-01-01), Machurat et al.
patent: 4206161 (1980-06-01), Sato et al.
patent: 4212837 (1980-07-01), Oguchi et al.
patent: 4219444 (1980-08-01), Hill et al.
patent: 4230832 (1980-10-01), Wei
patent: 4278576 (1981-07-01), Goldman
patent: 4289863 (1981-09-01), Hill
patent: 4311580 (1982-01-01), Bartholic
patent: 4328091 (1982-05-01), Bartholic
patent: 4346182 (1982-08-01), Gagliani et al.
patent: 4348301 (1982-09-01), Crompton et al.
patent: 4397968 (1983-08-01), Eck et al.
patent: 4397971 (1983-08-01), Hocker et al.
patent: 4427538 (1984-01-01), Bartholic
patent: 4446009 (1984-05-01), Bartholic
patent: 4460572 (1984-07-01), Derby et al.
patent: 4504529 (1985-03-01), Sorensen et al.
patent: 4518738 (1985-05-01), Sorensen et al.
patent: 4519939 (1985-05-01), Hecker et al.
patent: 4532295 (1985-07-01), Brabetz et al.
patent: 4537805 (1985-08-01), Lin et al.
patent: 4542184 (1985-09-01), Eck et al.
patent: 4560724 (1985-12-01), Brabetz et al.
patent: 4613639 (1986-09-01), Blum et al.
patent: 4617327 (1986-10-01), Podszun
patent: 4711748 (1987-12-01), Irwin et al.
patent: 4801411 (1989-01-01), Wellinghoff et al.
patent: 4863646 (1989-09-01), Watanabe et al.
patent: 4871489 (1989-10-01), Ketcham
patent: 4906699 (1990-03-01), Siol et al.
patent: 4923776 (1990-05-01), Hedvall et al.
patent: 4929400 (1990-05-01), Rembaum et al.
patent: 4999225 (1991-03-01), Rotolico
patent: 5008036 (1991-04-01), Crompton et al.
patent: 5015423 (1991-05-01), Eguchi et al.
Promotional flyer published by the National Institute of Standards and Technology in Gaithersburg, MD, offering for sale units of SRM 1960.
Levendis, Yiannis A., and Flagan, Richard C., "Combustion of Uniformly Sized Glassy Carbon Particles," Combust. Sci. and Tech., 1987, vol. 53, pp. 117-136.
Levendis, Yiannis A., and Flagan, Richard C., "Synthesis, Formation and Characterization of Micro-Sized Glassy Carbon Spheres of Controlled Pore Structure," Carbon, vol. 27, No. 2, pp. 265-283.
Flagan Richard
Levendis Yiannis A.
Panagiotou Thomai
Northeastern University
Theisen Mary Lynn
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