Production of methyldichlorophosphane

Details Production of methyldichlorophosphane Production of methyldichlorophosphane

1977-07-11

1978-08-01

Schwartz, Gerald A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07F 952, C07F 902

Patent

active

041043049

ABSTRACT:
Production of methyldichlorophosphane. The compound is made by reacting methane and phosphorus trichloride in a reaction zone in which a temperature higher than 500.degree. C is maintained. More specifically, hot reaction gas coming from the reaction zone is mechanically freed from solid matter, and the reaction gas freed from solid matter is passed to a quenching zone in which it is quenched with liquefied reaction mixture having 0.3 to 5 weight % of an organic barium compound or a non-ionic surfactant dissolved therein.

REFERENCES:
patent: 3210418 (1965-10-01), Pianfetti
Pianfetti et al., J. Am. Chem. Soc., vol. 84, pp. 851-854 (1962).

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