Production of highly capacitive agglomerated valve metal powder

Powder metallurgy processes – Powder metallurgy processes with heating or sintering – Making porous product

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419 30, 419 31, 419 44, 419 45, 75 05BB, 75 84, B22F 310, B22F 100, B22F 900

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044838190

ABSTRACT:
A process for the production of agglomerated valve metal powder which comprises heating an admixture of a valve metal powder and a reducing agent in the presence of an inert gas or under high vacuum for a sufficient time and at a sufficiently elevated temperature that agglomeration of the valve metal powder occurs, and removing the reaction products of the reducing agent and the valve metal and any unreacted reducing agent from the agglomerated valve metal powder by subsequent reaction with an inorganic acid. The agglomerated powder can be sintered to prepare valve metal electrodes, e.g., anodes, which can also be prepared by direct sintering of the admixture of the metal powder and the reducing agent.

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