Production of formate salts from carbon dioxide, hydrogen and am

Details Production of formate salts from carbon dioxide, hydrogen and am Production of formate salts from carbon dioxide, hydrogen and am

1983-05-16

1984-10-02

Berch, Mark L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitrogen attached directly or indirectly to the purine ring...

2602433, 2605011, 546348, 562609, 562550, C07C 5306, C07C 5115, C07D48708, C07D21318

Patent

active

044749597

ABSTRACT:
Formate salts of nitrogenous bases containing tertiary nitrogen are prepared by reacting the nitrogenous base with carbon dioxide and hydrogen using a soluble transition metal catalyst. For example triethylamine is reacted with carbon dioxide and hydrogen using ruthenium trichloride as catalyst and an isopropanol/water mixture as solvent to yield triethylammonium formate which was separated from the reaction mixture by distillation.

REFERENCES:
Inoue et al., J. Chem. Soc. Commun., 17, 718, (1975).
Inoue et al., Chem. Abs., 87, 67853, (1977).
Inoue et al., Chem. Lett., 8, 863-864, (1976).

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