Production of ethyl chlorothioformate

Details Production of ethyl chlorothioformate Production of ethyl chlorothioformate

1977-03-09

1978-10-10

Gotts, Lewis

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C15309

Patent

active

041196597

ABSTRACT:
An improved process for producing alkyl, lower cycloalkyl, lower cycloalkylmethyl, lower alkenyl, phenyl, benzyl, chloro-substituted phenyl and certain haloalkyl chlorothioformates by the reaction of the corresponding mercaptan with phosgene. The process is conducted in two stages, both occurring in a continuous liquid phase, in the presence of an activated carbon catalyst. Production of by-product disulfide is minimized and overall capacity can be increased.

REFERENCES:
patent: 3093537 (1963-06-01), Tilles
patent: 3165544 (1965-01-01), Tilles
patent: 3277143 (1966-10-01), Tilles

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