Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing
Patent
1995-03-17
1996-08-13
Burn, Brian M.
Organic compounds -- part of the class 532-570 series
Organic compounds
Amino nitrogen containing
564477, 564503, 564506, C07C20960
Patent
active
055457576
ABSTRACT:
A process for producing mixtures of mono-, di- and triethanol-amine by reacting ammonia and ethylene oxide in a cooled tubular reactor at temperatures from 110.degree. to 160.degree. C. and pressures from 50 to 120 bar comprises using ammonia and ethylene oxide in a molar ratio from 1:1 to 100:1 and ammonia in the form of a from 60 to 99.99% strength aqueous solution and adding from 1 to 80% of the ethylene oxide in from one to ten aliquots over from 10 to 70% of the total length of the tubular reactor.
REFERENCES:
patent: 3723530 (1973-03-01), Goetze et al.
patent: 4939301 (1990-07-01), Grice et al.
Chemical Abstracts 96 (1982) 51806g.
Hammer Hans
Reutemann Werner
BASF - Aktiengesellschaft
Burn Brian M.
Shurtleff John H.
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