Production of dodecahydrododecaborate (2-)

Details Production of dodecahydrododecaborate (2-) Production of dodecahydrododecaborate (2-)

1975-03-24

1976-06-01

Peters, G. O.

Chemistry of inorganic compounds

Boron or compound thereof

Hydrogen and metal or ammonium containing

C01B 3518

Patent

active

039610179

ABSTRACT:
This invention relates to the preparation of dodecahydrododecaborate (2-) anions and particularly to the preparation of alkali metal dodecahydrododecaborates such as Na.sub.2 B.sub.12 H.sub.12. The process of the invention involves the reaction of an alkali metal borohydride with dimethylsulfideborane, at a temperature and for a time sufficient, to yield the alkali metal dodecahydrododecaborate. The reaction may be conducted at atmospheric pressure.

REFERENCES:
patent: 3328134 (1967-06-01), Miller et al.
patent: 3882037 (1975-05-01), Brown
Adams, R. M., Boron Metallo-Boron Compounds and Boranes, Interscience Publishers, N.Y., 1964, p. 386.
Hughes, R. L. et al., Production of the Boranes and Related Research, Academic Press, N.Y., 1967, pp. 102-103.

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