Production of aralkyl tertiary hydroperoxides

Details Production of aralkyl tertiary hydroperoxides Production of aralkyl tertiary hydroperoxides

1976-04-01

1978-03-21

Thomas, Jr., James O.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260610A, C07C17902

Patent

active

040803864

ABSTRACT:
A portion of a recycle stream obtained as a result of the oxidation of an aryl tertiary alkane and containing aralkyl tertiary monohydroperoxide, substantial amounts of unreacted aryl tertiary alkane and lesser amounts of poly-oxy-functional oxidation by-products is subjected to aqueous alkaline extraction to remove at least a portion of the poly-oxy-functional oxidation by-products therefrom followed by separation of the extraction mixture into an aqueous alkaline phase and an organic phase, the organic phase being recycled to the oxidation reaction.

REFERENCES:
patent: 2715646 (1955-08-01), Hawkins
patent: 2856432 (1958-10-01), Conner et al.
patent: 2856433 (1958-10-01), Thompson
patent: 2915557 (1959-12-01), Kreps et al.
patent: 2915558 (1959-12-01), Alder et al.
patent: 3190923 (1965-06-01), Sodomann et al.
patent: 3190924 (1965-06-01), Sodomann et al.

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