Production of alkyl hypohalites

Details Production of alkyl hypohalites Production of alkyl hypohalites

1980-09-08

1982-08-03

Ford, John M.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C 6963

Patent

active

043427030

ABSTRACT:
Alkyl hypohalites are produced by reaction of tertiary alkanol with chlorine and aqueous base, or prechlorinated aqueous base, in a high back-mix recycle loop reactor operated at a recycle ratio of at least 5:1 to thereby control reaction temperature and permit the use of short reaction times; i.e., less than 5 minutes. The loop reactor is operated at a velocity sufficient to maintain a well dispersed reaction mixture of the organic, aqueous and gas phases.
Tertiary butyl hypochlorite is a preferred product.

REFERENCES:
patent: 1938175 (1933-12-01), Deanesly
patent: 3957442 (1976-05-01), Yamamoto et al.
patent: 4008133 (1977-02-01), Gelbein et al.

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