Producing phosphorus oxyhalide

Chemistry of inorganic compounds – Phosphorus or compound thereof – Halogen containing

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C01B 2510

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active

041839056

ABSTRACT:
Improvement in the oxidation of phosphorus trihalide to the oxyhalide in a reactor having a lower reaction zone and at least one upper reaction zone, whereby the trihalide is introduced at the bottom portion of the upper reaction zone and rises upwardly, reacting with oxygen fed in at the bottom portion of said lower reaction zone, the PX.sub.3 -POX.sub.3 mixture exits through exit means in the top portion of said upper reaction zone and is fed therethrough to the topmost portion of said lower reaction zone where said mixture flows downwardly toward the product exit and reacts with upwardly flowing suitable quality oxygen.

REFERENCES:
patent: 3052520 (1962-09-01), Draeger et al.
patent: 3956463 (1976-05-01), Winn, Jr.

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