Processes for preparation of 9,11-epoxy steroids and intermediat

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

540 43, 552502, 552508, C07J 1900, C07J 2100

Patent

active

059817445

ABSTRACT:
Multiple reaction schemes, process steps and intermediates are provided for the synthesis of epoxymexrenone, useful as a diuretic, and other 9,11-epoxy-steroids.

REFERENCES:
patent: 3053856 (1962-09-01), Payne et al.
patent: 3200113 (1965-08-01), Christiansen et al.
patent: 3300489 (1967-01-01), Holden
patent: 3413288 (1968-11-01), Creger
patent: 3759791 (1973-09-01), Marsheck
patent: 3897417 (1975-07-01), Warnant et al.
patent: 4118488 (1978-10-01), Philippson et al.
patent: 4559332 (1985-12-01), Grob et al.
patent: 5616742 (1997-04-01), Fu et al.
PCT Search Report Issued for PCT/US 96/20780 dated Sep. 22, 1997.
D.H.Peterson et al, "Microbiological Transformations of Steroids. VI. Preparation of 11.alpha.-Hydroxy-6-dehydro-progesterone", Journal of the American Chemical Society, vol. 75, No. 2, pp. 419-421, Jan. 29, 1953.
R. Christiansen et al., "The Reaction of Steroidal 4,6-dien-3-ones With Cyanide", Steroids, vol. 1, No. 6, pp. 620-627, Jun. 1963.
R.M. Weir et al., "7.alpha.-Carboalkoxy Steroidal Spirolactones As Aldosterone Antagonists", Journal of Medicinal Chemistry, vol. 18, No. 8, pp. 817-821, Aug. 1975.
C.M.P. Deshayes, "Utilisation De Modeles Mathematiques Pour l'optimisation En Fermentation. Applications Aux Transformations Par Les Micro-organismes", Bulletin De La Societe Chimique De France 2 Partie--Chimie Organique, Biochimie, No. 1-2, pp. 24-34, May 18, 1979.
Database WPI, Section Ch, Week 8145, Derwent Publications Ltd., London, GB; Class B01, AN 81-82258D and JP 56 120 697 A (Mitsubishi Chem. Ind. Ltd.), Sep. 22, 1981.
Abstract 084228, "Hydroxylated Androstane Production From Sterols" Chemical Abstracts, vol. 100, No. 11, p. 430, Mar. 12, 1984 and JP 58 179 498 A (Danippon Ink and Chemicals, Inc.; Japan, Oct. 20, 1983.
D. Van Leusen et al., "Chemistry Of Sulfonylmethyl Isocyanides. 33. Synthesis of 17-(isocyanotosylmethylene) Steroids: Precursors To Pregnane Derivatives" Recueil Des Travaux Chimiques Des Pays-Bas, vol. 110, No. 10, pp. 393-401, Oct. 1991.
Edward A. Brown, et al., J. Med. Chem, "Steroidal Aldosterone Blockers," 1963, vol. 6, pp. 732-735.
Brown et al., "Steroidal Aldosterone Blockers. III". J. Org. Chem., vol. 25(1), 1960.
Edward A. Brown, et al., Journal of Organic Chemistry, "Steroidal Aldosterone Blockers. III," 1960, vol. 25, No. 1, pp. 96-99.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Processes for preparation of 9,11-epoxy steroids and intermediat does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Processes for preparation of 9,11-epoxy steroids and intermediat, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Processes for preparation of 9,11-epoxy steroids and intermediat will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-1457852

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.