Process to produce oxygen and nitrogen at medium pressure

Refrigeration – Processes – Circulating external gas

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62 39, 62 41, F25J 302

Patent

active

051652447

ABSTRACT:
The present invention is an improvement to a process for the separation of air into its constituent components in a cryogenic distillation column system having a high pressure column and a low pressure column which are thermally integrated with each other. The improvement for producing both nitrogen and oxygen products at a medium pressure comprises the following steps: (a) operating the low pressure column at a pressure of between 10 to 75 psig and the high pressure column at a pressure which is about 60 to 160 psi higher than the low pressure column; (b) removing and subsequently warming at least a portion of the lower pressure nitrogen overhead from the top of the low pressure column and recovering the warmed, lower pressure nitrogen overhead portion as medium pressure gaseous nitrogen product; and (c) recovering medium pressure gaseous oxygen product from the low pressure column. There are two alternative ways to recover the medium pressure oxygen product of step (c). In the first, a portion of the liquid oxygen bottoms can be removed from the low pressure column and boosted in pressure, and then subsequently vaporized. This vaporized, boosted pressure, liquid oxygen is recovered as medium pressure gaseous oxygen product. In the second, a portion of the vaporized liquid oxygen bottoms is removed from the low pressure column and warmed. This warmed, vaporized liquid oxygen bottoms would be recovered as the medium pressure gaseous oxygen product.

REFERENCES:
patent: 2918802 (1959-12-01), Grunberg
patent: 3086371 (1963-04-01), Schilling et al.
patent: 4372764 (1983-02-01), Theobald
patent: 4617036 (1986-10-01), Suchdeo et al.
patent: 4790866 (1988-12-01), Rathbone

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