Process to produce 4-(2-sulfoethyl) cyclohexane, 1,2-diol...

Details Process to produce 4-(2-sulfoethyl) cyclohexane, 1,2-diol... Process to produce 4-(2-sulfoethyl) cyclohexane, 1,2-diol...

2005-06-14

2005-06-14

Barts, Samuel (Department: 1621)

Organic compounds -- part of the class 532-570 series

Organic compounds

Sulfonic acids or salts thereof

C562S109000, C562S115000, C562S030000

Reexamination Certificate

active

06906220

ABSTRACT:
Disclosed herein is a process for preparing 4-(2-sulfoethylcyclohexane)-1,2-diol sodium salt, at ambient condition and in the presence of a buffer and an initiator, from vinylcyclohexane-1,2-diol. Also disclosed is a process for preparing 3-(2-sulfoethyl) hexanedioic acid, sodium salt by oxidizing 4-(2-sulfoethylcyclohexane)-1,2 diol sodium salt with hydrogen peroxide in the presence of tungstic acid.

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Synthesis of Highly Water-Soluble Cyclodextrin Sulfonates by Addition of Hydrogen Sulfite to Cyclodextrin Allyl Ethers. Gerhard Wenz and Thomas Hofler. Carbohydrate Research 322 (1999) 153-165.
The Peroxide Effect in the Addition of Reagents to Unsaturated Compounds. IVIII. The Addition and Substitution of Bisulfite. M. S. Kharasch, Ernest M. May, and Frank R. Mayo. J. Org. Chem. v. 3, 1938-39, pp. 175-192.

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