Process of regenerating a noble metal catalyst used in the reduc

Compositions – Preservative agents – Anti-oxidants or chemical change inhibitants

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252413, 252414, 260575, 260689, B01J 2396, B01J 2120

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active

041644816

ABSTRACT:
Noble metal catalysts are regenerated according to a process comprising the steps of washing the deactivated catalyst with a polar organic solvent; contacting the washed catalyst with a hot aqueous alkali metal hydroxide solution; contacting the catalyst with an oxygen-containing gas at moderately elevated temperatures; and washing the catalyst a final time with a polar organic solvent. This method of regenerating the catalyst is particularly useful to reactivate palladium on carbon catalysts deactivated in the reduction of nitrophenol compounds to aminophenols.

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patent: 3959382 (1976-05-01), Yeh et al.
Chemical Abstracts - 81; 127336S, 1974, Matzuzawa et al., "Reclaiming a Catalyst by Treating with Aqueous Alkali, Oxidizing then Reducing".
Chem. Abs. - 81; 127337T, 1974, Matzuzawa et al., "Reclaiming a Catalyst by Treating with Aqueous Alkali and Reducing".

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