Process of producing XMX in 100% yield and purity

Details Process of producing XMX in 100% yield and purity Process of producing XMX in 100% yield and purity

1991-10-15

1992-06-23

Maples, John S.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

149 92, 149105, 149106, 540475, C07D25706

Patent

active

051244934

ABSTRACT:
An improvement when 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane is preed by nitrolysis of 1,3,5,7-tetraacyl-1,3,5,7-tetraazaceyloctane with a solution of nitric acid and nitrogen pentoxide or phosphorous pentoxide. This improved process herein before set forth produces 99% yield and purity of product.

REFERENCES:
patent: 3415868 (1968-12-01), Smetana et al.
patent: 3939148 (1976-02-01), Siele et al.
patent: 4432902 (1984-02-01), McGuire et al.
patent: 4534895 (1985-08-01), Frankel et al.
patent: 4614800 (1986-09-01), Willer et al.
patent: 4920859 (1989-04-01), Millar et al.

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