Process of producing pyrimidyl thiocarbonates

Details Process of producing pyrimidyl thiocarbonates Process of producing pyrimidyl thiocarbonates

1974-06-13

1976-02-03

Gotts, Lewis

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D23910

Patent

active

039364526

ABSTRACT:
Thiolcarbonates represented by the formula, ##SPC1##
Wherein R.sub.1 and R.sub.2 are individually a hydrogen atom or a methyl group, and R.sub.3 is a straight chain or branched chain saturated or unsaturated alkyl group having 1 to 5 carbon atoms or is a benzyl or benzhydryl group which may be nuclear substituted, are easily produced by reacting an alkali metal salt of 2-mercaptopyrimidine with phosgene, and reacting the resulting thiolchloroformate with an alcohol (R.sub.3 OH).

REFERENCES:
patent: 2923727 (1960-02-01), Neumoyer
patent: 3359296 (1967-12-01), Newallis et al.
patent: 3789061 (1974-01-01), Hoyer et al.
patent: 3855238 (1974-12-01), Batesky et al.
(Hoeben-Weyl), "Methoden Der Organischen Chemie", p. 808, (1955).

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