Process of preparing an amino thiazolyl disulfide using a water

Organic compounds -- part of the class 532-570 series – Organic compounds – Four or more ring nitrogens in the bicyclo ring system

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C07D41712

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040585247

ABSTRACT:
In a known process for preparing 2-(4-morpholinodithio)-benzothiazole using 2,2'-dithiobis(benzothiazole) along with morpholine, sulfur, an inert organic solvent such as isopropyl alcohol and an oxidizing agent, the improvement wherein a water soluble salt in combination with wet 2,2'-dithiobis(benzothiazole) is substituted for dry 2,2'-dithiobis(benzothiazole).

REFERENCES:
patent: 2837519 (1958-06-01), Hardman
patent: 3150130 (1964-09-01), Hardman
patent: 3178428 (1965-04-01), Eaker et al.
patent: 3281418 (1966-10-01), Budd et al.

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