Process of manufacturing improved polyurethane fiber polymer

Details Process of manufacturing improved polyurethane fiber polymer Process of manufacturing improved polyurethane fiber polymer

1996-07-24

1997-07-01

Foelak, Morton

Synthetic resins or natural rubbers -- part of the class 520 ser

Synthetic resins

From reactant having at least one -n=c=x group as well as...

528 61, 528906, C08G 1818, C08G 1832

Patent

active

056440154

ABSTRACT:
The present invention relates to a process of producing a polymer suitable for manufacturing spandex filament having remarkable elastic recovery rate and heat-setting efficiency wherein the process comprises: stirring a mixture of a glycol and a diisocyante, where the molar ratio of diisocyanate to glycol is 1.5 to 1.64, in a homogenizer at about 40.degree. to about 50.degree. C. and reacting said mixture to give a first polymer containing less than 4 mole % of unreacted diisocyanate; then, reacting said polymer with a chain-extender mixture containing ethylenediamine, 1,2-diaminopropane, and diethylenetriamine, preferably, about 74 to about 80 mole % of ethylenediamine, about 19 to about 25 mole % of 1,2-diaminopropane and about 0.2 to about 0.8 mole % of diethylenetriamine. Elastic polyurethaneurea-based spandex filament is produced by dry-spinning the polymer.

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