Process of discontinuous polycondensation and stirring...

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – Organic polymerization

Reexamination Certificate

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Details

C422S132000, C422S134000, C422S135000, C422S138000, C422S225000, C422S228000, C422S234000

Reexamination Certificate

active

07850926

ABSTRACT:
A process for the discontinuous production of granules from polycondensation polymers by precondensation of an oligomer at 5 to 400 mbar and subsequent polycondensation in a stirring reactor and subsequent granulation. In the vicinity of the outlet port, the density of the entraining surfaces lies between 1 and 8 m2per m3reactor space and constantly increases with increasing distance from the discharge region. Inside the reactor, there is a viscosity gradient between the region most remote from the discharge port and the zone of the discharge port. The thermal decomposition of the polymer melt flowing out of the reactor is compensated during granulation.The stirring reactor with horizontal longitudinal axis approximately has the shape of a single or double truncated cone. The reactor has rotatable, vertical product entraining surfaces and stationary scrapers between the same.

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