Process for working up cross-linked isocyanate distillation resi

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Cellular products or processes of preparing a cellular...

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260 9, 260 13, 260453AR, 260453SP, 521163, 521164, 521167, 525452, 525540, C08G 1814

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active

043118003

ABSTRACT:
This invention relates to the preparation of soluble compounds containing hydroxyalkyl and urethane groups by alcoholysis from highly cross-linked insoluble distillation residues (from the commercial production of tolylene diisocyanate) which have reacted completely or almost completely with water. The products obtained as solutions, solvent-free melts or powders may be used as raw materials for the production of synthetic resins or their intermediates which are characterized by reduced combustibility. They may also be recyclized by simple hydrolysis into the tolylene diamines ("TDA") from which tolylene diisocyanate ("TDI") is derived.

REFERENCES:
patent: 3128310 (1964-04-01), Koch
patent: 3331876 (1967-07-01), vanHorn et al.
patent: 3636030 (1972-01-01), Perkins
patent: 3897314 (1975-07-01), Liebsch et al.
patent: 4076577 (1978-02-01), Hetzel et al.
patent: 4105686 (1978-08-01), Raes et al.
patent: 4143008 (1979-03-01), Zwolinski et al.

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