Distillation: processes – separatory – Addition of material to distilland to inhibit or prevent... – For inhibiting or preventing a polymerization reaction
Patent
1982-06-28
1984-07-03
Bascomb, Jr., Wilbur L.
Distillation: processes, separatory
Addition of material to distilland to inhibit or prevent...
For inhibiting or preventing a polymerization reaction
203 65, 585 4, 585860, B01D 334, C07C 705, C07C 720
Patent
active
044578067
ABSTRACT:
This invention is directed to the use of a polymerization inhibitor in the distillation of readily polymerizable vinyl aromatic monomers and more specifically to the use of mixtures of 2,6-dinitro-4-ethyl-phenol as a polymerization inhibitor for vinyl aromatic monomers such as styrene and vinyl benzenes. The invention comprises the process of subjecting the vinyl aromatic monomers to distillation temperatures in the presence of mixtures of 2,6-dinitro-4-ethyl-phenol and 2,6-dinitro-paracresol to prevent polymerization.
REFERENCES:
patent: 2526567 (1950-10-01), Drake et al.
patent: 4033829 (1977-07-01), Higgins et al.
patent: 4105506 (1978-08-01), Watson
patent: 4182658 (1980-01-01), Watson
patent: 4252615 (1981-02-01), Watson
Grivas John C.
Park Myong-Gi A.
Bascomb, Jr. Wilbur L.
McDonald Robert E.
The Sherwin-Williams Company
Tura James V.
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