Process for the synthesis of tetradecahydroundecaborate compound

Details Process for the synthesis of tetradecahydroundecaborate compound Process for the synthesis of tetradecahydroundecaborate compound

1977-09-29

1978-09-19

Peters, G. O.

Chemistry of inorganic compounds

Boron or compound thereof

Hydrogen and metal or ammonium containing

423286, 423294, C01B 3518

Patent

active

041155203

ABSTRACT:
Tetradecahydroundecaborate compounds, MB.sub.11 H.sub.14, wherein M represents a monovalent cation are prepared by the reaction of the corresponding octahydroborate compounds, MB.sub.3 H.sub.8, with boron trifluoride. The reaction is carried out at a temperature of 100.degree. C. to 120.degree. C., preferably in an inert solvent medium.

REFERENCES:
patent: 3328134 (1967-06-01), Miller et al.
patent: 3458531 (1969-07-01), Aftandilian
patent: 3489517 (1970-01-01), Shore et al.

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