Process for the synthesis of bis(alkyl sulphide)-decaborane (12)

Details Process for the synthesis of bis(alkyl sulphide)-decaborane (12) Process for the synthesis of bis(alkyl sulphide)-decaborane (12)

1977-10-11

1979-06-19

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07F 502

Patent

active

041586735

ABSTRACT:
The invention relates to a process for the synthesis of bis(alkyl sulphide)-decaboranes (12).
This synthesis is characterized in that a decahydrodecaborate (2-) salt of the general formula M.sub.2 B.sub.10 H.sub.10, in which M represents a positive radical, is treated with a mixture comprising a strong oxygen-containing acid and an alkyl sulphide of the formula R.sub.2 S, in which R is a lower alkyl radical. In a preferred procedure, the said mixture is a solution of a strong oxygen-containing acid which is saturated with an alkyl sulphide.
The bis(alkyl sulphide)-decaboranes (12) are especially useful in the synthesis of certain carboranes.

REFERENCES:
patent: 3154561 (1964-10-01), Muetterties
patent: 3296260 (1967-01-01), Knoth
patent: 3489812 (1970-01-01), Marshall et al.

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