Process for the synthesis of 2,4,6,8-tetranitro-2,4,6,8-tetraaza

Details Process for the synthesis of 2,4,6,8-tetranitro-2,4,6,8-tetraaza Process for the synthesis of 2,4,6,8-tetranitro-2,4,6,8-tetraaza

1995-02-21

1997-08-19

Jordan, Charles T.

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitrogen attached directly or indirectly to the purine ring...

C07D47100

Patent

active

056590326

ABSTRACT:
The invention relates to a new process for the synthesis of 2,4,6,8-tetranitro-2,4,6,8-tetraazabicyclo-[3.3.0]octane (bicyclo-HMX) by reaction of nitronium tetrafluoroborate with 2,4,6,8-tetraacetyl-2,4,6,8-tetraazabicyclo[3.3.0]octane in the presence of fluoride ions.
The process makes it possible to obtain pure bicyclo-HMX in an acceptable yield.
Bicyclo-HMX is an explosive which can be employed as explosive or propellent charge in solid pyrotechnic compositions.

REFERENCES:
patent: 4443602 (1984-04-01), Willer
patent: 4503299 (1985-03-01), Willer
patent: 4614800 (1986-09-01), Willer
Coon Cliff, "Synthesis of Energetic Materials", Energetic & Technology Review, Jan. Feb. 1988.
Adolph et al, "Synthesis of Energetic Materials" Annual Progress Report for the Office of Naval Research Mar. 1984.

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