Process for the removal of ammonium sulphate from tarrich waste

Chemistry of inorganic compounds – Sulfur or compound thereof – Oxygen containing

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208 13, 210723, 23302A, C01C 124

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051417324

ABSTRACT:
The ammonium sulphate contained in tar-rich waste streams from the production of (meth)acrylonitrile can be precipitated out by adding 1 to 30 times the amount by weight of methanol, relative to the water content of the waste stream, and additionally 0.05 to 10% the amount by weight of ammonia, relative to methanol, to such a waste stream at 10.degree.-60.degree. C. and separating off the ammonium sulphate which precipitates out. The waste stream remaining after separating off the ammonium sulphate can, for example, be disposed of as low-sulphur waste-fuel in a combustion chamber.

REFERENCES:
patent: 3408157 (1968-10-01), Miller et al.
patent: 3902859 (1975-09-01), Greco
Chemical Abstracts, vol. 88, 1978, paragraph No. 123360s, Columbus, Ohio, US: & JP-A-52 153 899 (Ube Industries) 21.12.1977.

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